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Reasons from interfacial thermodynamics, Langmuir/BET/D-R adsorption, and Young–Dupré wetting through XPS (ISO 15472/18118, AdC vacuum-level alignment, SESSA), contact-angle SFE (OWRK/vOCG, ASTM D7490), QCM-D viscoelastic modeling, ToF-SIMS, SAMs, and ISO 20579 handling while treating adventitious carbon, charging, siloxane contamination, Cassie–Wenzel states, and tip convolution as first-class failure modes.